HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 43167782, compound → HCID 86592113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 43167782 | HCID 43167782 | — |
| Reactant | Ethyl 2-[(2-ethylbutyl)amino]nicotinate | HCID 67064133 | — |
| Product | HCID 86592113 | HCID 86592113 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 3B substituting the product of Example 71A for the product of Example 3A (0.205 g, 55%). MS (ESI+) m/z 249.1 (M+H)+; 1H NMR (300 MHz, CDCl3) δ 1.63 (m, 6H), 1.84 (m, 4H), 2.43 (m, 2H), 5.39 (s, 1H), 7.24 (dd, J=7.72, 4.78 Hz, 1H), 8.40 (m, 1H), 8.71 (dd, J=4.78, 1.84 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902203B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-5dc2a01c624c4212b37ce443be261898 |
| Source note | uspto-grants-2011_03 |