Butyl bromide → HCID 11680572, compound

HRID 601133Notes

Reaction equation

C(Br)CCC.[Cl:6][C:7]1[C:12]2[C:13](=[O:18])[O:14][C:15](=[O:17])[NH:16][C:11]=2[CH:10]=[CH:9][CH:8]=1.N1[C:24]2N=C[CH:27]=[CH:28][C:23]=2[C:22](=O)OC1=O>>[Cl:6][C:7]1[C:12]2[C:13](=[O:18])[O:14][C:15](=[O:17])[N:16]([CH2:27][CH2:28][CH:23]([CH3:24])[CH3:22])[C:11]=2[CH:10]=[CH:9][CH:8]=1

Participants

Reactant 3

HCID 8002Butyl bromide

HCID 6390585-chloro-2,4-dihydro-1H-3,1-benzoxazine-2,4-dione

HCID 109865823-Azaisatoic anhydride

Product 1

HCID 11680572HCID 11680572, compound

Procedure

The title compound was prepared according to the procedure of Example 1B substituting 1-bromo-3-methylbutane for n-butyl bromide and substituting the product of Example 101A for the product of Example 1A (0.610 g, 45%). MS (DCI) m/z 285 (M+NH4)+.

Sources & evidence

ORD record: ord-5b59c532972846959fc6805e791045a4
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07902203B2

Reaction notes

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