HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-aminocyclohex-1-ene-1-carboxylate → 5,6,7,8-tetrahydro-2H-3,1-benzoxazine-2,4(1H)-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-aminocyclohex-1-ene-1-carboxylate | HCID 312929 | — |
| Reactant | Ethyl 2-[(2-ethylbutyl)amino]nicotinate | HCID 67064133 | — |
| Product | 5,6,7,8-tetrahydro-2H-3,1-benzoxazine-2,4(1H)-dione | HCID 13809650 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 3B substituting ethyl 2-aminocyclohex-1-ene-1-carboxylate for the product of Example 3A (0.960 g, 97%). MS (ESI−) m/z 166 (M−H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902203B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-be9104209980441490f19aced8f83fa6 |
| Source note | uspto-grants-2011_03 |