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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 601145Generated: October 30, 2026

Ammonia → HCID 86592119, compound

https://huagongshe.com/reaction/601145

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantBenzyl BromideHCID 7498—
ReactantButyl bromideHCID 8002—
Reactant3-Azaisatoic anhydrideHCID 10986582—
ProductHCID 86592119HCID 86592119—

Reaction Steps

The title compound was prepared according to the procedure of Example 1B substituting the product of Example 123A for the product of Example 1A and substituting benzyl bromide for n-butyl bromide (0.109 g, 27%). MS (DCI/NH3) m/z 249 (M+NH4)+; 1H NMR (300 MHz, DMSO-d6) δ 1.86 (s, 3 H) 2.14 (s, 3 H) 5.09 (s, 2 H) 7.32 (m, 5 H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07902203B2
Source datasetuspto-grants-2011_03
ORD IDord-14cc614b3401495e9e4c04334eb465cc
Source noteuspto-grants-2011_03