Ammonia → HCID 86592119, compound

HRID 601145Notes

Reaction equation

HRID 601145 reaction equation
[NH:1]1[C:6]2N=CC=[CH:10][C:5]=2[C:4](=[O:11])[O:3][C:2]1=[O:12].[CH2:13](Br)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[CH2:21](Br)CCC.N>>[CH2:13]([N:1]1[C:6]([CH3:21])=[C:5]([CH3:10])[C:4](=[O:11])[O:3][C:2]1=[O:12])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

5

Reactant 4

HCID 222AmmoniaHCID 7498Benzyl BromideHCID 8002Butyl bromideHCID 109865823-Azaisatoic anhydride

Product 1

HCID 86592119HCID 86592119, compound

Procedure

The title compound was prepared according to the procedure of Example 1B substituting the product of Example 123A for the product of Example 1A and substituting benzyl bromide for n-butyl bromide (0.109 g, 27%). MS (DCI/NH3) m/z 249 (M+NH4)+; 1H NMR (300 MHz, DMSO-d6) δ 1.86 (s, 3 H) 2.14 (s, 3 H) 5.09 (s, 2 H) 7.32 (m, 5 H).

Sources & evidence

ORD record
ord-14cc614b3401495e9e4c04334eb465cc
Source dataset
uspto-grants-2011_03
Patent number
US07902203B2

Reaction notes

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