HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl bromide → HCID 85967349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl bromide | HCID 8002 | — |
| Reactant | Pentane, 3-(bromomethyl)- | HCID 77432 | — |
| Reactant | 3-Azaisatoic anhydride | HCID 10986582 | — |
| Product | HCID 85967349 | HCID 85967349 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 1B substituting the product of Example 123A for the product of Example 1A and substituting 1-bromo-2-ethyl-butane for n-butyl bromide (0.181 g, 45%). 1H NMR (300 MHz, DMSO-d6) δ 0.85 (t, J=7.35 Hz, 6 H) 1.29 (m, 4 H) 1.65 (m, 1 H) 1.86 (s, 3 H) 2.25 (s, 3 H) 3.73 (d, J=7.35 Hz, 2 H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902203B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-533d25d4d9bf4a48824f33b61f2e1339 |
| Source note | uspto-grants-2011_03 |