Butyl bromide → HCID 85967349, compound

HRID 601148Notes

Reaction equation

[NH:1]1[C:6]2N=CC=[CH:10][C:5]=2[C:4](=[O:11])[O:3][C:2]1=[O:12].Br[CH2:14][CH:15]([CH2:18][CH3:19])[CH2:16][CH3:17].[CH2:20](Br)CCC>>[CH2:16]([CH:15]([CH2:18][CH3:19])[CH2:14][N:1]1[C:6]([CH3:20])=[C:5]([CH3:10])[C:4](=[O:11])[O:3][C:2]1=[O:12])[CH3:17]

Participants

Reactant 3

HCID 8002Butyl bromide

HCID 77432Pentane, 3-(bromomethyl)-

HCID 109865823-Azaisatoic anhydride

Product 1

HCID 85967349HCID 85967349, compound

Procedure

The title compound was prepared according to the procedure of Example 1B substituting the product of Example 123A for the product of Example 1A and substituting 1-bromo-2-ethyl-butane for n-butyl bromide (0.181 g, 45%). 1H NMR (300 MHz, DMSO-d6) δ 0.85 (t, J=7.35 Hz, 6 H) 1.29 (m, 4 H) 1.65 (m, 1 H) 1.86 (s, 3 H) 2.25 (s, 3 H) 3.73 (d, J=7.35 Hz, 2 H).

Sources & evidence

ORD record: ord-533d25d4d9bf4a48824f33b61f2e1339
Source dataset: uspto-grants-2011_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07902203B2

Reaction notes

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