HRID60142

反应详情

EQUATION

反应方程式

HRID 60142 的结构方程式

PROCEDURE

实验过程

Concentrated hydrochloric acid (0.16 ml) was added to an aqueous solution (2 ml) of the sodium 2-(4-fluorophenyl)-5,6,7,8-tetrahydro-[1,2,4]triazolo[1,5-a]pyridine-7-carboxylate (530 mg) obtained in (Example 5.2) <Step 2>, and the obtained mixture was then stirred for 15 minutes. Thereafter, the precipitated solid was collected by filtration, so as to obtain the title compound (196 mg) in the form of a whitish brown solid.

WORKUP

后处理

  1. customobtained in (Example 5.2) <Step 2>
  2. filtrationThereafter, the precipitated solid was collected by filtration