HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Bromide → HCID 86600820, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Bromide | HCID 6332 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | HCID 67290352 | HCID 67290352 | — |
| Product | HCID 86600820 | HCID 86600820 | — |
Reaction Steps
Ethylbromide (7.5 ml) is added to a solution of terephthalic acid bis-{1-[1-(3-dimethylamino-propylcarbamoyl)ethoxy]-2,6-diethyl-2,3,6-trimethyl-piperidine-4-yl} ester (11.0 g, 0.0125 mol) in acetonitrile (20 ml). The mixture is stirred at room temperature for 17 h and is then evaporated to afford 14.1 g of the title compound as a colorless amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902368B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-38d88f74491841e0bb3bd88eda8263a6 |
| Source note | uspto-grants-2011_03 |