HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 11349506, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 11439986 | HCID 11439986 | — |
| Catalyst | Methyl iodide | HCID 6328 | — |
| Product | HCID 11349506 | HCID 11349506 | — |
Reaction Steps
At room temperature, 3 mg of 60% of sodium hydride was added to 1 ml solution of dimethylformamide with 10 mg of 1-(2-fluoropyridine-3-yl)-4-(1-oxo-2-methylcarbonyloxy-indane-5-yl)-5-methyl-1H-[1,2,3]triazole, obtained in Example 45. After stirring 30 min at room temperature, 5 drops of methyl iodide was added and the mixture was further stirred for 1 hour at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902369B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-90217c9637f14ba696263e31c0ffd11f |
| Source note | uspto-grants-2011_03 |