Methyl iodide → HCID 23158207, compound

Participants

Reaction Steps

640 mg of 60% of sodium hydroxide was added at room temperature to 20 ml solution of dimethylformamide with 850 mg of 5-bromo-2-methylcarbonyloxy-1-indanone obtained in the above 1). After stirring for 10 min at room temperature, 3.5 ml of methyl iodide was added and the mixture was stirred for 1 hour at room temperature. Then, 2 ml of dimethylformamide containing 5% water was added and further stirred for 1 hour at room temperature.

Provenance & Evidence