Triethylamine → HCID 23158109, compound

Participants

Reaction Steps

10 mg of the compound obtained in Example 217 was dissolved in 2 ml of chloroform, 20 μl of methanesulfonylchloride and 20 μl of triethylamine were added, and after 30 min at room temperature, the solvents were distilled outunder reduced pressure. The obtained residues were purified by silicagel thin-layer chromatography (ethyl acetate) to obtain 12.3 mg of the above compound as a white solid.

Provenance & Evidence