HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → HCID 59180203, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | 3-TETRAHYDROPYRANYLOXY-1-TRIMETHYLSILYL-1-PROPYNE | HCID 10703781 | — |
| Product | HCID 59180203 | HCID 59180203 | — |
Reaction Steps
Reaction of trimethyl(3-(tetrahydro-2H-pyran-2-yloxy)prop-1-ynyl)silane (4.6 g, 21.6 mmol 4.6 g, 21.6 mmol) and (z)-5-bromo-pent-3-enyl)-benzene, (4.1 g, 18 mmol)) according to General Procedure 11.A provided the title compound. The material was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902252B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-7051f465bf504a7ea2e82cc3ff77213f |
| Source note | uspto-grants-2011_03 |