HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Biphenylcarboxylic acid, 4'-chloro- → HCID 58992583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Biphenylcarboxylic acid, 4'-chloro- | HCID 616002 | — |
| Reactant | HCID 58992672 | HCID 58992672 | — |
| Product | HCID 58992583 | HCID 58992583 | 82.3% |
Reaction Steps
Using methyl 3-[3-(aminomethyl)piperidin-1-yl]benzoate (76.2 mg, 0.307 mmol) and 4′-chlorobiphenyl-4-carboxylic acid (77.2 mg, 0.332 mmol), the same procedure was followed as in Step 61e of Example 61 to give 117 mg (82%) of the desired compound as a pale yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07902367B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-64b5c4387a9d4abd84ae286c6f923938 |
| Source note | uspto-grants-2011_03 |