Hydrochloric Acid → HCID 178438345, compound

HRID 602246Notes

Reaction equation

HRID 602246 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH:47]=[O:48])[N:5]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:23]3[N:27](C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)[N:26]=[N:25][N:24]=3)=[CH:13][CH:12]=2)[C:6]=1[CH2:7][CH2:8][CH3:9].Cl>>[Br:1][C:2]1[CH:3]=[C:4]([CH:47]=[O:48])[N:5]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:23]3[NH:27][N:26]=[N:25][N:24]=3)=[CH:13][CH:12]=2)[C:6]=1[CH2:7][CH2:8][CH3:9]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86615717HCID 86615717, compound

Product 1

HCID 178438345HCID 178438345, compoundYield 52%

Procedure

This compound was prepared using the same procedure as in Example 1.10 g of 4-bromo-5-n-propyl-1-[2′-(1-triphenylmethyltetrazol-5-yl)biphenyl-4-yl-methyl]-2-pyrrolaldehyde (0.015 moles) and 19 mL of 4N HCl (0.075 moles) yield 3.5 g of product. Formula: C22H20BrN5O (m.w. 450.34). Yield 52%.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-3dd576c53d4d4bf4bc5750e2adb8d800
Source dataset
uspto-grants-2011_03
Patent number
US07906501B2

Reaction notes

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