Hydrochloric Acid → HCID 178439357, compound

HRID 602248Notes

Reaction equation

HRID 602248 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:47]=[O:48])[N:5]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:23]3[N:27](C(C4C=CC=CC=4)(C4C=CC=CC=4)C4C=CC=CC=4)[N:26]=[N:25][N:24]=3)=[CH:13][CH:12]=2)[C:6]=1[CH2:7][CH2:8][CH3:9].Cl>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:47]=[O:48])[N:5]([CH2:10][C:11]2[CH:16]=[CH:15][C:14]([C:17]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:23]3[NH:27][N:26]=[N:25][N:24]=3)=[CH:13][CH:12]=2)[C:6]=1[CH2:7][CH2:8][CH3:9]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86615719HCID 86615719, compound

Product 1

HCID 178439357HCID 178439357, compoundYield 65%

Procedure

This compound was prepared using the same procedure as in Example 1.12 g of 4-chloro-5-n-propyl-1-[2′-(1-triphenylmethyltetrazol-5-yl)biphenyl-4-yl-methyl]-2-pyrrolaldehyde (0.019 moles) and 24 mL of 4N HCl (0.095 moles) yield 5.0 g of product. Formula: C22H20ClN5O (m.w. 405.89). Yield 65%.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-b1f1312446134e6e9f61417a66b85ff0
Source dataset
uspto-grants-2011_03
Patent number
US07906501B2

Reaction notes

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