Hydrochloric Acid → HCID 178439188, compound

Participants

Reaction Conditions

Reaction Steps

100 mg of compound 2 (0.269 mmol) are dissolved in 50 mL of 0.1 N NaOH and 158 mL (1.6 mmol) of 35% H2O2 are added. The mixture is left to stand at ambient temperature for 18 h. The mixture is cooled to 0° C. and adjusted to pH 2 with 2N HCl. The solid is filtered out and washed with water. Drying is performed in a vacuum oven at 40° C. Product: 54 mg. Formula: C22H21N5O2 (m.w. 387.43). Yield 52%.

Provenance & Evidence