Hydrochloric Acid → HCID 44517825, compound

HRID 602630Notes

Reaction equation

HRID 602630 reaction equation
[C@@H:1]12[CH2:6][C@@H:5]1[CH2:4][N:3]([CH2:7][CH2:8][CH2:9][O:10][C:11]1[CH:19]=[CH:18][C:14]([C:15]([NH2:17])=[O:16])=[CH:13][CH:12]=1)[CH2:2]2.[ClH:20]>C(O)C>[ClH:20].[C@@H:5]12[CH2:6][C@@H:1]1[CH2:2][N:3]([CH2:7][CH2:8][CH2:9][O:10][C:11]1[CH:19]=[CH:18][C:14]([C:15]([NH2:17])=[O:16])=[CH:13][CH:12]=1)[CH2:4]2

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 445178264-{3-[(1R,5S)-3-Azabicyclo[3.1.0]hex-3-yl]propoxy}benzamide

Product 1

HCID 44517825HCID 44517825, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The product obtained in Step 2 is dissolved in 10 ml of ethanol, to which there are added 2 ml of 2N ethereal HCl solution. The crystallised product is filtered off, rinsed with ethanol and dried in vacuo.

Workup

  1. filtrationThe crystallised product is filtered off
  2. washrinsed with ethanol
  3. customdried in vacuo

Sources & evidence

ORD record
ord-6fb6b521e7fe45749d65df7b1bfc3baf
Source dataset
uspto-grants-2011_03
Patent number
US07906547B2

Reaction notes

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