HCID 67055305, compound → HCID 86609773, compound

HRID 602715Notes

Reaction equation

HRID 602715 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([C:9](=[C:15]2[CH2:18][N:17]([CH:19]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)[C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[CH2:16]2)[C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[C:6]([F:8])[CH:7]=1>C1COCC1>[CH2:13]([O:12][C:10](=[O:11])[CH:9]([C:4]1[CH:5]=[C:6]([F:8])[CH:7]=[C:2]([Br:1])[CH:3]=1)[CH:15]1[CH2:18][N:17]([CH:19]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[C:20]2[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=2)[CH2:16]1)[CH3:14]

Participants

3

Reactant 1

HCID 67055305HCID 67055305, compound

Product 1

HCID 86609773HCID 86609773, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The title compound was prepared from ethyl (3-bromo-5-fluorophenyl)[1-(diphenylmethyl)azetidin-3-ylidene]acetate according to the procedure described in Preparation 6 except that THF was used as the co-solvent; Mass Spectrum: m/e=482 (M+1, 79Br), 484 (M+1, 81Br).

Sources & evidence

ORD record
ord-bdff2b460f4c43b7b30c87e3a8ab0598
Source dataset
uspto-grants-2011_03
Patent number
US07906503B2

Reaction notes

Loading…