1-Naphthalenemethanamine → HCID 62368325, compound

HRID 602736Notes

Reaction equation

HRID 602736 reaction equation
[NH2:1][CH2:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1.[NH:13]([C:15](=[O:20])[C:16](OC)=[O:17])[NH2:14]>CO>[NH:13]([C:15](=[O:20])[C:16]([NH:1][CH2:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[CH:6]=[CH:5][CH:4]=1)=[O:17])[NH2:14]

Participants

4

Reactant 2

HCID 83551-NaphthalenemethanamineHCID 11355473Methyl hydrazino(oxo)acetate

Product 1

HCID 62368325HCID 62368325, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent2×

Procedure

1.25 ml 1-aminomethylnaphthalene are added to a solution of 1.0 g methyl hydrazino-oxo-acetate in 10 ml of methanol. The solution is stirred for 16 h at ambient temperature and then some of the methanol is eliminated. The precipitate is separated off, washed with diethyl ether, and dried.

Workup

  1. customThe precipitate is separated off
  2. washwashed with diethyl ether
  3. customdried

Sources & evidence

ORD record
ord-c722f2a7878444bc810ae6e8910dc318
Source dataset
uspto-grants-2011_03
Patent number
US07906539B2

Reaction notes

Loading…