HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenemethanamine → HCID 62368325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenemethanamine | HCID 8355 | — |
| Reactant | Methyl hydrazino(oxo)acetate | HCID 11355473 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 62368325 | HCID 62368325 | — |
Reaction Steps
1.25 ml 1-aminomethylnaphthalene are added to a solution of 1.0 g methyl hydrazino-oxo-acetate in 10 ml of methanol. The solution is stirred for 16 h at ambient temperature and then some of the methanol is eliminated. The precipitate is separated off, washed with diethyl ether, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07906539B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-c722f2a7878444bc810ae6e8910dc318 |
| Source note | uspto-grants-2011_03 |