HRID602829

反应详情

EQUATION

反应方程式

HRID 602829 的结构方程式

PROCEDURE

实验过程

Methanol (70 mL) was added dropwise under stirring at 0° C. to thionyl chloride (23.4 mL), and azetidine-3-carboxylic acid (CAS No. 36476-78-5, 25 g) was added, followed by stirring at room temperature for 2 hours. The reaction solution was concentrated, to thereby obtain the title compound (36 g) having the following physical properties.

WORKUP

后处理

  1. addition36476-78-5, 25 g) was added
  2. concentrationThe reaction solution was concentrated