HCID 67055305, compound → HCID 86609773, compound

HRID 602981Notes

Reaction equation

HRID 602981 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([C:9](=[C:15]2[CH2:18][N:17]([CH:19]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)[C:20]3[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=3)[CH2:16]2)[C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[C:6]([F:8])[CH:7]=1>C1COCC1>[Br:1][C:2]1[CH:3]=[C:4]([CH:9]([CH:15]2[CH2:18][N:17]([CH:19]([C:26]3[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=3)[C:20]3[CH:21]=[CH:22][CH:23]=[CH:24][CH:25]=3)[CH2:16]2)[C:10]([O:12][CH2:13][CH3:14])=[O:11])[CH:5]=[C:6]([F:8])[CH:7]=1

Participants

3

Reactant 1

HCID 67055305HCID 67055305, compound

Product 1

HCID 86609773HCID 86609773, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The title compound was prepared from ethyl (3-bromo-5-fluorophenyl)[1-(diphenylmethyl) azetidin-3-ylidene]acetate according to the procedure described in Preparation 6 except that THF was used as the co-solvent; Mass Spectrum: m/e=482 (M+1, 79Br), 484 (M+1, 81Br).

Sources & evidence

ORD record
ord-87029186b58944cfa4d9d664d2148a89
Source dataset
uspto-grants-2011_03
Patent number
US07906652B2

Reaction notes

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