Thionyl Chloride → 2,6-Dimethylbenzyl Chloride

HRID 603325Notes

Reaction equation

HRID 603325 reaction equation
[CH3:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[C:3]=1[CH2:4]O.S(Cl)([Cl:13])=O>>[CH3:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([CH3:10])[C:3]=1[CH2:4][Cl:13]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 186748(2,6-Dimethylphenyl)methanol

Product 1

HCID 2211542,6-Dimethylbenzyl Chloride

Procedure

To a stirred solution of 2,6-Dimethylbenzyl alcohol (9.94 g, 73 mmol) was added thionyl chloride (81.55 g, 685 mmol) at room temperature. The reaction mixture was stirred for 6 hours, concentrated under reduced pressure and used without further purification.

Workup

  1. concentrationconcentrated under reduced pressure
  2. customused without further purification

Sources & evidence

ORD record
ord-dcb34f05e4f04f489b0e4f253533796d
Source dataset
uspto-grants-2011_03
Patent number
US07906675B2

Reaction notes

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