HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 2,6-Dimethylbenzyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (2,6-Dimethylphenyl)methanol | HCID 186748 | — |
| Product | 2,6-Dimethylbenzyl Chloride | HCID 221154 | — |
Reaction Steps
To a stirred solution of 2,6-Dimethylbenzyl alcohol (9.94 g, 73 mmol) was added thionyl chloride (81.55 g, 685 mmol) at room temperature. The reaction mixture was stirred for 6 hours, concentrated under reduced pressure and used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07906675B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-dcb34f05e4f04f489b0e4f253533796d |
| Source note | uspto-grants-2011_03 |