HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluidine → HCID 178426386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluidine | HCID 7813 | — |
| Reactant | Tert-butyl 2-(4-formylphenoxy)acetate | HCID 639902 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178426386 | HCID 178426386 | — |
Reaction Steps
tert-Butyl (4-formylphenoxy)acetate (5.0 g, 21.2 mmol) was dissolved in dry toluene (100 mL) and p-toluidine (2.27 g, 21.2 mmol) was added. The mixture was refluxed in a Dean-Stark apparatus for 18 hours, cooled and concentrated under reduced pressure. Heptane was added and the mixture was concentrated under reduced pressure. This afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07906502B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-7e08c27e3a1548faaee68adffb568624 |
| Source note | uspto-grants-2011_03 |