Urea → HCID 178517731, compound

Participants

Reaction Steps

10 mmol of 4 are dissolved in 100 ml of aqueous ethanol and mixed with 25 mmol of urea. It is refluxed for 7 h, the solvent is removed and the colorless solid is washed with water. Recrystallization from chloroform gives 20 in a yield above 90%. ESI MS, m/z (%): 366.3703 (100) [M+H]+. 31P{1H} NMR (101.2 MHz, 25° C., DMSO-d6): 5-7.45.

Provenance & Evidence