Hydroquinone → HCID 57174946, compound

HRID 605093Notes

Reaction equation

HRID 605093 reaction equation
Cl[C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=1[N+:11]([O-:13])=[O:12].[C:14]1([CH:21]=[CH:20][C:18]([OH:19])=[CH:17][CH:16]=1)[OH:15]>>[OH:15][C:14]1[CH:21]=[CH:20][C:18]([O:19][C:2]2[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[CH:4][C:3]=2[N+:11]([O-:13])=[O:12])=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 785HydroquinoneHCID 73204-Chloro-3-nitrobenzoic acid

Product 1

HCID 57174946HCID 57174946, compound

Procedure

A mixture of 4-chloro-3-nitrobenzoic acid was reacted with hydroquinone to produce 4-(4-Hydroxy-phenoxy)-3-nitro-benzoic acid according to the procedure of Example 37A, which was treated sequentially with Benzyl-methyl-amine using the procedure from Example 37B and reduced using the procedure from Example 37C to provide the title product.

Sources & evidence

ORD record
ord-30b5748c486c4ddcb5b555354fc8b0fe
Source dataset
uspto-grants-2011_03
Patent number
US07910595B2

Reaction notes

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