HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoroaniline → HCID 67040494, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoroaniline | HCID 9584 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 86615545 | HCID 86615545 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67040494 | HCID 67040494 | — |
Reaction Steps
A solution of the product from Example 43D (53 mg, 0.1 mmol), N,N-diisopropylethylamine (0.052 mL, 0.3 mmol), 2-Fluoro-phenylamine (0.014 mL, 0.15 mmol) in dichloromethane (2 mL) was stirred at room temperature for 1 hour, then concentrated under vacuum to provide the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-c6656169a4764329a84642a733dc1654 |
| Source note | uspto-grants-2011_03 |