HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-5-fluoropyridine → 4-Fluoro-N-(5-fluoro-pyridin-2-yl)-3-nitro-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-5-fluoropyridine | HCID 2737701 | — |
| Reactant | 4-Fluoro-3-nitrobenzoyl chloride | HCID 2783347 | — |
| Product | 4-Fluoro-N-(5-fluoro-pyridin-2-yl)-3-nitro-benzamide | HCID 63236206 | 98% |
Reaction Steps
The product from Example 172a was reacted with 5-Fluoro-pyridin-2-ylamine (165 mg, 1.474 mmol) according to the procedure from Example 172a to provide the title compound (404 mg, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-4d6b36906a434091b7586babc95d131b |
| Source note | uspto-grants-2011_03 |