HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3,4-Thiadiazol-2-amine → 4-Fluoro-3-nitro-N-[1,3,4]thiadiazol-2-yl-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3,4-Thiadiazol-2-amine | HCID 19909 | — |
| Reactant | 4-Fluoro-3-nitrobenzoyl chloride | HCID 2783347 | — |
| Product | 4-Fluoro-3-nitro-N-[1,3,4]thiadiazol-2-yl-benzamide | HCID 43216610 | 67% |
Reaction Steps
The product from Example 172a was reacted with [1,3,4]Thiadiazol-2-ylamine (149 mg, 1.474 mmol) according to the procedure from Example 172b to provide the title compound (272 mg, 67%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-ed2f5c9026ea4eb8a679630cac026aa2 |
| Source note | uspto-grants-2011_03 |