4-Methylbenzenethiol → HCID 67040447, compound

Participants

Reaction Conditions

Reaction Steps

The product from Example 242b (600 mg, 1.828 mmol) was dissolved in DMF (20 mL) to which K2CO3 (505 mg, 3.656 mmol), and 4-methyl-benzenethiol (227 mg, 1.828 mmol) were added. This reaction mixture was then heated to 80° C. for 1 hr. At this time the reaction mixture was cooled to room temperature, diluted with water, and the title compound collected by filtration (611 mg, 77

Provenance & Evidence