HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 67040477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Cesium carbonate | HCID 10796 | — |
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Reactant | HCID 56763846 | HCID 56763846 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 67040477 | HCID 67040477 | — |
Reaction Steps
The product from Example 351A (1 equiv) and 4-mercaptophenol (1 equiv) were dissolved in dimethylformamide and cesium carbonate (5 equiv) added. The resultant mixture was stirred at 80° C. for 2.5 hours, cooled to room temperature and water added. The solution was extracted with ethyl acetate, the organic extracts dried and concentrated under vacuum to provide the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07910595B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-149745779bac4c5f9a7501b9b1308c5e |
| Source note | uspto-grants-2011_03 |