HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 3-[(3R,4R)-3,4-Dimethylpiperidin-4-yl]phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 67690602 | HCID 67690602 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-[(3R,4R)-3,4-Dimethylpiperidin-4-yl]phenol | HCID 11052767 | — |
Reaction Steps
A beaker was charged with methanol (0.4 kg), water (0.5 L), and Compound 7(100 g). The mixture was charged to the reactor and rinsed forward with a solution of water (0.3 L) and methanol (0.2 kg) to seed the reaction mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07914776B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-45b3388f9abd4e1e8a39f2ff1324fc4d |
| Source note | uspto-grants-2011_03 |