Aluminum → Sucrose

HRID 605447Notes

Reaction equation

HRID 605447 reaction equation
[CH2:1]([OH:23])[C@H:2]1[O:6][C@:5]([O:9][C@H:10]2[O:15][CH:14]([CH2:16][OH:17])[C@@H:13]([OH:18])[C@H:12]([OH:19])[CH:11]2[OH:20])([CH2:7][OH:8])[CH:4]([OH:21])[C@H:3]1[OH:22].[Al]>O>[CH2:16]([OH:17])[C@H:14]1[O:15][C@H:10]([O:9][C@:5]2([CH2:7][OH:8])[O:6][C@H:2]([CH2:1][OH:23])[C@@H:3]([OH:22])[C@@H:4]2[OH:21])[C@H:11]([OH:20])[C@@H:12]([OH:19])[C@@H:13]1[OH:18]

Participants

4

Reactant 2

HCID 5359268AluminumHCID 46782954HCID 46782954, compound2×

Product 1

HCID 5988Sucrose

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A Sucrose/Lake red dye (Opalux Red AS-1662-D, available from Colorcon, West Point, Pa.) solution was prepared by mixing 966.3 g of sucrose NF into 414.7 g of purified water in a stainless steel container using a magnetic stir bar. The container was covered with aluminum foil and heated to about 60—about 65° C. with continued mixing. The solution was mixed for an additional 20 minutes at about 60—about 65° C. at which time the solution was visually clear. 9.2 g of lake red dye was added to the sucrose NF solution, the foil replaced, and mixing continued for 10 minutes while maintaining temperature between about 60—about 65° C.

Workup

  1. temperatureheated to about 60—about 65° C. with continued mixing
  2. additionThe solution was mixed for an additional 20 minutes at about 60—about 65° C. at which time the solution
  3. additionmixing
  4. temperaturewhile maintaining temperature between about 60—about 65° C.

Sources & evidence

ORD record
ord-58b1e600a98c4034a17e949cf0e61f46
Source dataset
uspto-grants-2011_03
Patent number
US07914811B2

Reaction notes

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