HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butoxy bis(dimethylamino)methane → HCID 53423662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butoxy bis(dimethylamino)methane | HCID 79885 | — |
| Reactant | 1-(4-Chlorophenyl)-3,3-dimethylbutan-2-one | HCID 10104569 | — |
| Product | HCID 53423662 | HCID 53423662 | — |
Reaction Steps
1-(4-Chlorophenyl)-3,3-dimethyl-butan-2-one (30 mmol) and tert-butoxybis-(dimethylamino)methane (31.5 mmol) are heated together at reflux overnight. The reaction mixture is then cooled to RT and the excess tert-butoxybis(dimethylamino)methane removed under reduced pressure to give 2-(4-chlorophenyl)-1-dimethylamino-4,4-dimethyl-pent-1-en-3-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915264B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-28901e7a217948939c71802d2eb0773b |
| Source note | uspto-grants-2011_03 |