HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → (5-phenylisoxazol-3-yl)methylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 17473432 | HCID 17473432 | — |
| Product | (5-phenylisoxazol-3-yl)methylamine | HCID 5200315 | — |
Reaction Steps
2-[(5-Phenylisoxazol-3-yl)methyl]-1H-isoindole-1,3(2H)-dione (3.48 g, 11.4 mmol) was treated with hydrazine hydrate (1.35 g, 22.9 mmol) according to the method described in Part E of Example 35 to provide (5-phenylisoxazol-3-yl)methylamine as a pale yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915281B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-c6b2f48cd79a40bcac189b9549856a77 |
| Source note | uspto-grants-2011_03 |