HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → Piperidinium, 1-methyl-4-oxo-1-(phenylmethyl)-, bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 1-Methyl-4-piperidone | HCID 74049 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Piperidinium, 1-methyl-4-oxo-1-(phenylmethyl)-, bromide | HCID 10802960 | — |
Reaction Steps
To a solution of 1-methyl-4-piperidinone (15 g, 132.6 mmol) in dry acetone (100 mL) was added 1-bromomethylbenzene (24.9 g, 145 mmol) dropwise. It was stirred for 3 h. The title compound (116) separated which was filtered, washed with dry acetone and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915301B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-27e1b8da45184bc6857d2f5550f04015 |
| Source note | uspto-grants-2011_03 |