HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[(4-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}butyl)oxy]benzonitrile → 1-{3-[(4-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}butyl)oxy]phenyl}methanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[(4-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}butyl)oxy]benzonitrile | HCID 66769081 | — |
| Reactant | 3-[(3-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}propyl)oxy]benzonitrile | HCID 66769189 | — |
| Product | 1-{3-[(4-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}butyl)oxy]phenyl}methanamine | HCID 66768258 | — |
Reaction Steps
By a method similar to that in Reference Example 7 and using, instead of 3-[(3-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}propyl)oxy]benzonitrile, 3-[(4-{[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]thio}butyl)oxy]benzonitrile obtained in Reference Example 10, the title compound was obtained as a yellow oil (8.65 g, 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915267B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-2b0571b767924271990ffdc76141cc19 |
| Source note | uspto-grants-2011_03 |