HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl 1-trityl-1H-1,2,4-triazole-3-carboxylate → (1-trityl-1H-1,2,4-triazol-3-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl 1-trityl-1H-1,2,4-triazole-3-carboxylate | HCID 58739241 | — |
| Reactant | ethyl 3-[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]propanoate | HCID 66769033 | — |
| Product | (1-trityl-1H-1,2,4-triazol-3-yl)methanol | HCID 13471694 | — |
Reaction Steps
By a method similar to that in Reference Example 26 and using, instead of ethyl 3-[1-(triphenylmethyl)-1H-1,2,4-triazol-3-yl]propanoate, methyl 1-(triphenylmethyl)-1H-1,2,4-triazole-3-carboxylate obtained in Reference Example 34, the title compound was obtained as a white powder (5.35 g, 58%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915267B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-f1a4c30d480a4073a812c8abfcb109ef |
| Source note | uspto-grants-2011_03 |