HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-4-fluorobenzene → HCID 67047602, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-4-fluorobenzene | HCID 522627 | — |
| Reactant | 3-Bromo-5-methylpyridine | HCID 817713 | — |
| Product | HCID 67047602 | HCID 67047602 | 25% |
Reaction Steps
Prepare essentially as described in PREPARATION 10 using 3-bromo-5-methylpyridine, (prepared as described in PREPARATION 1), (196 mg, 1.14 mmol) and 1-ethynyl-4-fluorobenzene (150 mg, 1.25 mmol) to give the title compound (60 mg, 25%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-5a57fa40d9334946884cbeded77ff887 |
| Source note | uspto-grants-2011_03 |