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HRID606857

反应详情

EQUATION

反应方程式

HRID 606857 的结构方程式

REACTANTS

反应物

2
结构：C#Cc1cccc([N+](=O)[O-])c1
HCID76432

3-Nitrophenylacetylene

C8H5NO2

结构：N#Cc1cncc(Br)c1
HCID736793

5-bromonicotinonitrile

C6H3BrN2

PRODUCTS

生成物

1
结构：N#Cc1cncc(C#Cc2cccc([N+](=O)[O-])c2)c1
HCID67047684

未命名化合物

收率 65%

PROCEDURE

实验过程

Prepare essentially as described in PREPARATION 10 using 5-bromonicotinonitrile (400 mg, 2.19 mmol) and 1-ethynyl-3-nitrobenzene, (prepared as described in PREPARATION 11), (644 mg, 4.38 mmol) to give the title compound (118 mg, 65%).

WORKUP

后处理

  1. customPrepare essentially