HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Iodophenol → 5-(3-Hydroxyphenylethynyl)-nicotinonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Iodophenol | HCID 12272 | — |
| Reactant | 5-Ethynylnicotinonitrile | HCID 22416563 | — |
| Product | 5-(3-Hydroxyphenylethynyl)-nicotinonitrile | HCID 67047546 | 17% |
Reaction Steps
Prepare essentially as described in EXAMPLE 10 using 3-iodophenol (0.69 g, 3.0 mmol) and 5-ethynylnicotinonitrile (0.4 g, 3.0 mmol) to give the title compound (110 mg, 17%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-0aa0978605eb4a59b7d0246e7861106d |
| Source note | uspto-grants-2011_03 |