HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-CHLORO-4-IODO-1-METHOXYBENZENE → HCID 67047660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-CHLORO-4-IODO-1-METHOXYBENZENE | HCID 11184750 | — |
| Reactant | 5-[2-(Trimethylsilyl)ethynyl]pyridine-3-carbonitrile | HCID 16115699 | — |
| Product | HCID 67047660 | HCID 67047660 | 174.4% |
Reaction Steps
Prepare according to the general procedure outlined in EXAMPLE 72 using 2-chloro-4-iodo-1-methoxybenzene (520 mg, 19 mmol) and 5-trimethylsilanylethynyl-nicotinonitrile (350 mg, 1.75 mmol), (prepared as described in PREPARATION 3), to give the title compound (820 mg, 47%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-b4898ee671af4d5ab44e52e0527d46be |
| Source note | uspto-grants-2011_03 |