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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 606881Generated: October 31, 2026

Potassium Carbonate → HCID 86622477, compound

https://huagongshe.com/reaction/606881

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantO-Methylhydroxylamine hydrochlorideHCID 521874—
ReactantHCID 86076475HCID 86076475—
ProductHCID 86622477HCID 8662247780%

Reaction Steps

Prepare in a similar manner as described in EXAMPLE 6 using 5-(3,4-difluorophenylethynyl)-pyridine-3-carbaldehyde, (prepared essentially as described in EXAMPLE 101), (0.28 g, 1.15 mmol), methoxylamine hydrochloride (0.77 g, 9.21 mmol) and potassium carbonate (0.80 g, 5.76 mmol) to give the title compound (0.28 g, 80%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07915424B2
Source datasetuspto-grants-2011_03
ORD IDord-63cf2c8c23854425a53683f8c5a70190
Source noteuspto-grants-2011_03