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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 606882Generated: October 30, 2026

Potassium Carbonate → HCID 86622479, compound

https://huagongshe.com/reaction/606882

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantHCID 86076475HCID 86076475—
ProductHCID 86622479HCID 8662247935.4%

Reaction Steps

Prepare in a similar manner as described in EXAMPLE 6 using 5-(3,4-difluorophenylethynyl)-pyridine-3-carbaldehyde (0.28 g, 1.15 mmol), (prepared essentially as described in EXAMPLE 101), hydroxylamine hydrochloride (0.64 g, 9.21 mmol) and potassium carbonate (0.80 g, 5.76 mmol) to give the title compound (0.120 g, 35%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07915424B2
Source datasetuspto-grants-2011_03
ORD IDord-81141734d0224c359a473d08a6a09a0b
Source noteuspto-grants-2011_03