HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 86622479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 86076475 | HCID 86076475 | — |
| Product | HCID 86622479 | HCID 86622479 | 35.4% |
Reaction Steps
Prepare in a similar manner as described in EXAMPLE 6 using 5-(3,4-difluorophenylethynyl)-pyridine-3-carbaldehyde (0.28 g, 1.15 mmol), (prepared essentially as described in EXAMPLE 101), hydroxylamine hydrochloride (0.64 g, 9.21 mmol) and potassium carbonate (0.80 g, 5.76 mmol) to give the title compound (0.120 g, 35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-81141734d0224c359a473d08a6a09a0b |
| Source note | uspto-grants-2011_03 |