HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → HCID 67047779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | HCID 67048040 | HCID 67048040 | — |
| Product | HCID 67047779 | HCID 67047779 | 49% |
Reaction Steps
Prepare essentially as described in EXAMPLE 158 using 5-(3-trifluoromethylphenylethynyl)-pyridin-3-ylamine hydrochloride, (prepared as described in EXAMPLE 155), (151 mg, 0.45 mmol) and methyl chloroformate (0.03 mL, 0.45 mmol) to give the title compound (70 mg, 49%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-ed0cd82f9e304c5ca53fc9de592d9efa |
| Source note | uspto-grants-2011_03 |