HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1-fluoro-2-nitrobenzene → HCID 67047647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1-fluoro-2-nitrobenzene | HCID 2736328 | — |
| Reactant | 5-Ethynylnicotinonitrile | HCID 22416563 | — |
| Product | HCID 67047647 | HCID 67047647 | 9.1% |
Reaction Steps
Prepare essentially as described in EXAMPLE 142 using 4-bromo-1-fluoro -2-nitrobenzene (1.0 g, 4.5 mmol) and 5-ethynylnicotinonitrile, (prepared as described in PREPARATION 4), (0.7 g, 5.5 mmol) to give the title compound as a yellow solid (0.11 g, 9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-58b4211942c947a48ba15e398837dbcc |
| Source note | uspto-grants-2011_03 |