HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67047742, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67047667 | HCID 67047667 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 67047742 | HCID 67047742 | 93% |
Reaction Steps
Add 1 M hydrogen chloride in diethyl ether (0.61 mL, 1.1 eq) to a solution of 5-phenylethynyl-nicotinic acid methyl ester, (prepared as described in EXAMPLE 173), (0.15 g, 0.56 mmol) in diethyl ether and stir at room temperature for 2 h. Isolate the precipitated solid by filtration to give the title compound (0.16 g, 93%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915424B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-3aa148525f06485ab93048d342839986 |
| Source note | uspto-grants-2011_03 |