HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → HCID 66808558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 66808444 | HCID 66808444 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 66808558 | HCID 66808558 | — |
Reaction Steps
To the product from Example 181B (0.5 g, 2.0 mmol) in dichloromethane was treated with boron tribromide (10 mmol) at room temperature for 1 hour. The solution was the extracted with water, then the organic solution dried and concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07915411B2 |
| Source dataset | uspto-grants-2011_03 |
| ORD ID | ord-38509a7750704952b1ee54cbdca2e7fd |
| Source note | uspto-grants-2011_03 |